Harrick Praying Mantis 螳螂™ 高温反应室对于具有高比表面积的粉末特别有效。这使得漫反射成为研究多相催化、气固相互作用、光化学反应和氧化机制的有价值的工具。这种高温反应室非常适合在精心控制的温度和压力下进行此类研究。高温反应室应用允许在受控压力和广泛温度下进行漫反射（漂移）光谱测量。它和螳螂一起使用™ 红外光谱和紫外-可见漫反射光谱的附件。也可用于拉曼光谱。
特征
设计用于从高真空（133μPa或10-6torr）到133kpa（1ktorr），带KBr窗口或1.5mpa（11.3ktorr）带ZnSe窗口的操作。
达到910°C的温度（在真空下）。
易于适应高达3.44MPa（25.8ktorr）的操作，带有可选的高压圆顶。
提供三个入口/出口，用于排空电池和引入气体。
由耐化学腐蚀的316不锈钢制成。
可选的Silcotek/Restek惰性涂层可提高惰性和耐腐蚀性。
可选的冷却筒可用于中等程度的冷却或加热，带有冷却器或再循环装置。
可用于显微光谱应用的替代窗口组件，包括拉曼。
包括
反应室。
低压加热筒。
K型热电偶。
样品包装工具和溢液盘。
带有两个KBr或ZnSe窗口和一个玻璃观察窗口（FTIR配置）的圆顶。
带有两个SiO2窗口和一个玻璃观察窗口（UV-Vis-NIR配置）的圆顶。
相关配件：
| MODEL NO. | NAME | DESCRIPTION | |
|---|---|---|---|
| ATK-024-3 | Temperature Controller, 110V | Temperature Controller (110V) with USB to RS-485 Adapter | |
| ATK-024-4 | Temperature Controller, 220/240V | Temperature Controller (220/240V) with USB to RS-485 Adapter | |
| CHC-CHA-3 | Praying Mantis™ Low Temperature Reaction Chambers (FTIR) | Praying Mantis™ diffuse reflection environmental chamber, 24V | |
| CHC-VUV-3 | Praying Mantis™ Low Temperature Reaction Chambers (UV-Vis-NIR) | Praying Mantis™ diffuse reflection environmental chamber, 24V | |
| DRK-3-XXX | Diffuse Reflection Catalysis Package, 110V | Kit with Praying Mantis, Reaction Chamber, Controller, etc. | |
| DRK-4-XXX | Diffuse Reflection Catalysis Package, 220V | Kit with Praying Mantis, Reaction Chamber, Controller, etc. | |
| DRP-XXX | Praying Mantis™ Diffuse Reflection Accessory | Diffuse reflection accessory |
| MODEL NO. | NAME | |
|---|---|---|
| 007-085 | VCO to Swagelok Adapter (English) | |
| 116-998 | VCO to Swagelok Adapter (Metric) | |
| DRP-ASC | Ambient Chamber (FTIR) for Praying Mantis | |
| DRP-ASC-VUV | Ambient Chamber (UV-Vis-NIR) for Praying Mantis | |
| DRP-PDR | Praying Mantis Purge Shield | |
| HVC-COL | HVC Cooling Cartridge | |
| HVC-DWA-2 | Standard Reaction Chamber Dome, SiO₂ | |
| HVC-DWA-3 | High Press. Dome, SiO₂, for High Temp. Chamber | |
| HVC-DWI-2 | Standard Reaction Chamber Dome, ZnS | |
| HVC-DWI-3 | High Press. Dome, ZnS, for High Temp. Chamber | |
| HVC-DWM-2 | Standard Reaction Chamber Dome, ZnSe | |
| HVC-DWM-3 | High Press. Dome, ZnSe, for High Temp. Chamber | |
| HVC-DWP-2 | Standard Reaction Chamber Dome, KBr | |
| HVC-MRA | Standard Reaction Chamber Raman Assembly, SiO₂ |
易耗配件：
| MODEL NO. | NAME | ||
|---|---|---|---|
| 008-144 | Thermocouple, K-Type | ||
| 116-439 | Screen Set (2 each of the three sizes), 6.3 mm dia. | ||
| 116-439-1S | Screen Set (6), pore size 0.104 mm (0.0041″), 6.3 mm dia. | ||
| 116-439-2S | Screen Set (6), pore size 0.061 mm (0.0024″), 6.3 mm dia. | ||
| 116-439-3S | Screen Set (6), pore size 0.038 mm (0.0015″), 6.3 mm dia. | ||
| HVC-CER | Ceramic Filters (4, 80um max. pore dia), 6.3 mm dia. | ||
| KIT-SCP | Spatula/Scoopula |
| MODEL NO. | NAME | ||
|---|---|---|---|
| 116-429 | PTFE Washer, OD 0.59″ (15mm) |
|
|||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| MODEL NO. | NAME | ||
|---|---|---|---|
| HVC-ORK | Kalrez O-Rings for High Temp. Reaction Chambers | ||
| HVC-ORV | Viton O-Rings for High Temp. Reaction Chambers | ||
| ORK-010 | Kalrez O-Ring, 0.379 OD, 0.239 ID | ||
| ORK-013 | Kalrez O-Ring, 0.566 OD, 0.426 ID | ||
| ORK-016 | Kalrez O-Ring, 0.754 OD, 0.614 ID | ||
| ORK-023 | Kalrez O-Ring, 1.191 OD, 1.051 ID | ||
| ORV-010 | Viton O-Ring, 0.379 OD, 0.239 ID | ||
| ORV-013 | Viton O-Ring, 0.566 OD (15 mm), 0.426 ID | ||
| ORV-016 | Viton O-Ring, 0.754 OD, 0.614 ID | ||
| ORV-023 | Viton O-Ring, 1.191 OD, 1.051 ID |
| MODEL NO. | NAME | ||
|---|---|---|---|
| KBR-100 | KBr Powder, Spectroscopic Grade, 100 g |
| MODEL NO. | NAME | ||
|---|---|---|---|
| WAD-U23 | Window SiO₂ 15 x 2 mm | ||
| WAD-U43 | Window SiO₂ 15 x 4 mm | ||
| WED-U23 | Window Si 15 x 2 mm | ||
| WFD-U23 | Window CaF₂ 15 x 2 mm | ||
| WHD-U23 | Window BaF₂ 15 x 2 mm | ||
| WID-U43 | Window ZnS 15 x 4 mm | ||
| WJD-U23 | Window Ge 15 x 2 mm | ||
| WLD-U23 | Window NaCl 15 x 2 mm | ||
| WMD-U23 | Window ZnSe 15 x 2 mm | ||
| WMD-U43 | Window ZnSe 15 x 4 mm | ||
| WPD-U23 | Window KBr 15 x 2 mm |
